Modern Molecular Photochemistry Of Organic Molecules Pdf _VERIFIED_

Modern Molecular Photochemistry Of Organic Molecules Pdf _VERIFIED_





             

Modern Molecular Photochemistry Of Organic Molecules Pdf


CHEM-730: Nuclear Magnetic Resonance Spectroscopy Concepts and applications of NMR. NMR applied to organic chemistry. Spectroscopy: explanation of the line shapes of the nuclei in the spectrometer through Lorentz equations. Pulse techniques: Nuclear magnetic resonance spectroscopy. NMR methods: Selective irradiation, coherence, chemical shift, NOE, spin-lattice relaxation and spin-spin relaxation (T1, T2, T1ρ, and T2ρ). Experimental conditions: Spectrometer and sample parameters; reference measurements; spin count; temperature; line width; operating frequency; pulse duration. Recommended Books
1. C.A. Pound and E. Brink, Nuclear Magnetic Resonance, The Chemical Society, Oxford (1962)
2. K.F. Schuhmann, Magnetic Resonance in Chemistry, John Wiley and Sons (1999)

CHEM-718: Chemistry of Biological Systems
General: General chemistry of biological systems. Recombination of electrons and holes: mechanisms, analysis, characterisation, problems and prospects. Alkaloids, nucleic acids, proteins, carbohydrates and lipids. Molecular recognition mechanisms and applications. Binding of molecules: ligand binding to receptors. Quantitative aspects. Anti-microbial and anti-viral agents: synthesis and properties of different molecules. Quantitative aspects. Immunology: General aspects, immune system, vaccination and immunotherapy, molecular basis of transplant rejection and immunomodulation. Endocrine systems: synthesis of biogenic amines, serotonin, dopamine, histamine and their receptors. Quantitative aspects. Hormones and Signaling: different hormones and their mechanisms of action. Hormones and their interactions. Autocoids and peptides: autocoids and vasopressins. Endogenous peptides and their effects. Diseases and Pathogens: different infectious diseases. The molecular basis of drug resistance. Chemical evolution of biomacromolecules. Pharmacodynamics and pharmacokinetics: biodynamics of drug metabolism and pharmacokinetics of drugs. Metabolism of xenobiotics. Quantitative aspects.
Recommended Books
1. G. Hagen and C. Guenthner, Biosynthesis, Chemistry and Biology of Hormones, 3rd ed., Wiley-VCH, Weinheim, (1995)
2. P.B. Lowe, Principles and Applications of Organic Chemistry, 2nd ed., Wiley-Interscience, New York (2000)
3. S.R. Bechtel and P.V. Richer, Principles of Medicinal Chemistry, 5th ed., Academic Press, San Diego (1996)
4. D.L. Richman and K.R. Foster, Medicinal and Pharmaceutical Chemistry, Wiley-VCH, Weinheim (2004)




CHEM-719: Synthetic and Analytical Chemistry of Inorganic Materials Introduction: Analytical aspects of inorganic materials: preparation, characterisation and analysis of inorganic materials. Synthetic methods: nucleation and growth, solid-solid reactions, hydrometallurgy, the different phase-transition reactions in metals and alloys, synthesis of metal clusters and nanoparticles, sol-gel methods, the different preparation of new materials. Characterisation of inorganic materials: preparation, characterisation and analysis of inorganic materials. The preparation of new materials for organic chemistry, materials chemistry and analytical chemistry of inorganic materials CHEM-721: Inorganic Photochemistry Introduction: inorganic photochemistry, Application of photoacution and photolysis with different ligands and metals. CHEM-706: Assignment of 1H and 13C NMR spectra Typical results for preassigned 1H and 13C NMR spectra 1.1 Introduction: Preassigned one-dimensional 1H and 13C NMR spectra and the determination of 1H and 13C chemical shifts. 1.2 1H NMR Spectrum of uracil-5-carboxylic acid: Chemical shifts, multiplicities and coupling constant of protons and carbons; identification of signal positions and assignments; carbons in CH=C groups. 1.3 Experimental procedure for the determination of protons and carbons in CH=C groups: 1H and 13C NMR spectrum of the diacids of the monomeric and polymeric polycarboxylic acids; peak integration for the 1H and 13C NMR peaks of CH=C. 1.4 Hydrogens in CH=C groups: Non-exchangeable H at the carbonyl C and C adjacent to the carbonyl C. 1.5 Basic principles for the analysis of 1H NMR spectra in general: Analysis of one-dimensional 1H NMR spectra, estimation of chemical shifts, primary and secondary carbon substituents and stereochemistry. 1.6 Assignments of 1H NMR spectra of non-crystalline organic materials by 1D 1H NMR spectroscopy in D2O: Different types of carbon-containing moieties, group identities and number of protonated carbons. 1.7 Carbon substituents in 1H NMR spectra of crystalline organic materials: Aromatic 1H NMR spectra, protonation at C=O bonds, substitution at C=O bonds; acetate. 1.8 Assignment of 1H NMR spectra of organic materials by 2D NMR spectroscopy: 1H 1J 13C-COSY, 13C 1J 1H-COSY, 1H-1H 2J HETCOR and HMBC experiments; 1H NMR spectra of polymers; 1H NMR spectra of monomers, polymers and macromolecules. 5ec8ef588b


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